毛細(xì)管柱1：GS-GASPRO  30M*0.32MM

毛細(xì)管柱2：FFAP(聚乙二醇類）30m*0.32mm*0.25um

本標(biāo)準(zhǔn)規(guī)定了焦?fàn)t煤氣中硫化氫含量的氣相色譜測(cè)定的原理、儀器和材料、采樣、分析步驟、結(jié)果計(jì)算、度和安全注意事項(xiàng)。
本標(biāo)準(zhǔn)適用于焦?fàn)t煤氣中硫化氫含量的測(cè)定。

定量：外標(biāo)法

檢測(cè)器：FPD火焰光度檢測(cè)器

滕州市浩瀚色譜儀器技術(shù)服務(wù)有限公司，采用浩瀚色譜E公司帶FPD檢測(cè)器的GC-型氣相色譜儀測(cè)定了焦?fàn)t煤氣中H2S的含量,同時(shí)用國(guó)標(biāo)的碘滴定法進(jìn)行試驗(yàn)數(shù)據(jù)對(duì)比。結(jié)果表明,本方法分析周期由每樣2 h縮短到10 min左右,且煤氣中H2S的含量在（5～5 000）×10^-6的范圍內(nèi)線性關(guān)系良好,準(zhǔn)確度高,重現(xiàn)性好,完全滿足不同含量H2S分析要求,是一種簡(jiǎn)便快速的分析方法。


氣相色譜法分析焦?fàn)t煤氣中H2S 圖片：


Analysis of H2S in Coke Oven Gas by Gas Chromatography
Gas Chromatography Analysis of H2S in Coke Oven Gas Details:

Capillary column 1: GS-GASPRO 30M*0.32MM
Capillary column 2: FFAP (polyethylene glycol) 30m*0.32mm*0.25um

This standard specifies the principles, instruments and materials, sampling, analysis procedures, calculation of results, precision and safety precautions for the determination of hydrogen sulfide in coke oven gas.
This standard applies to the determination of hydrogen sulfide content in coke oven gas.
Quantification: external standard method
Detector: FPD flame photometric detector

Tengzhou Haohao Chromatography Instrument Technology Service Co., Ltd. measured the H2S content in coke oven gas by GC- gas chromatograph with FPD detector from Haohao Chromatography E Co., Ltd., and compared the test data with the national standard iodine titration method. The results show that the analysis period of this method is shortened from 2 h to 10 min, and the H2S content in the gas is in the range of (5～5 000)×10^-6. The linear relationship is good, the accuracy is high, and the reproducibility Well, fully meet the H2S analysis requirements of different levels, it is a simple and rapid analysis method.


Analysis of H2S in Coke Oven Gas by Gas Chromatography