名稱：毛細管柱
固定液：5%苯基+95%甲基聚硅氧烷

規(guī)格：30m*0.25mm*0.25um

型號：SE-54

應(yīng)用：GB/T 31407-2015 化妝品中碘丙炔醇丁基氨甲酸酯的測定 氣相色譜法

浩瀚色譜（山東）應(yīng)用技術(shù)開發(fā)有限公司建立護膚品面膜中碘丙炔醇丁基氨甲酸酯的氣相色譜-質(zhì)譜聯(lián)用的測定方法。方法樣品用乙醚提取,超聲15min,3 500r/min離心15min,提取液過無水硫酸鈉脫水,濃縮,殘渣用1.0mL丙酮定容,進行氣相色譜-質(zhì)譜法測定,經(jīng)SE-54色譜柱(30m×0.25mm,0.25μm)分離后,SIM掃描模式,外標(biāo)法定量。結(jié)果碘丙炔醇丁基氨甲酸酯在濃度0.1~10μg/mL范圍線性關(guān)系良好(r=0.999 3);在0.5~1.5μg/g添加水平范圍內(nèi),回收率為90.0%~94.67%,相對標(biāo)準(zhǔn)偏差(RSD)為3.4%~5.4%;檢出限(LOD)為0.01μg/g,定量限(LOQ)為0.05μg/g。結(jié)論該方法簡便、快速,重現(xiàn)性好,適用于護膚品面膜中碘丙炔醇丁基氨甲酸酯的測定。

測定化妝品中碘丙炔醇丁基氨甲酸酯 測試譜圖：



Determination of iodopropynol butyl carbamate in cosmetics
Determination of iodopropynol butyl carbamate in cosmetics

Name: Capillary Column
Fixing fluid: 5% phenyl + 95% methyl polysiloxane

Specification: 30m*0.25mm*0.25um

Model: SE-54

Application: GB/T 31407-2015 Determination of Iodopropynol Butyl Carbamate in Cosmetics Gas Chromatography

Haohan Chromatography (Shandong) Applied Technology Development Co., Ltd. established a gas chromatography-mass spectrometry method for the determination of iodopropynol butyl carbamate in facial masks of skin care products. Method The sample was extracted with ether, ultrasonic for 15min, and centrifuged at 3 500r/min for 15min. The extract was dehydrated by anhydrous sodium sulfate and concentrated. The residue was fixed to volume with 1.0mL acetone, and the gas chromatography-mass spectrometry was carried out. 30m×0.25mm, 0.25μm) after separation, SIM scanning mode, external standard method for quantification. Results Iodopropynol butyl carbamate has a good linear relationship in the concentration range of 0.1-10 μg/mL (r=0.999 3); in the range of 0.5-1.5 μg/g addition level, the recovery rate is 90.0%-94.67%. The relative standard deviation (RSD) is 3.4%~5.4%; the limit of detection (LOD) is 0.01 μg/g, and the limit of quantification (LOQ) is 0.05 μg/g. Conclusion The method is simple, rapid and reproducible. It is suitable for the determination of iodopropynol butyl carbamate in facial masks of skin care products.

Determination of iodopropynol butyl carbamate in cosmetics Test spectrum: