名稱：毛細管柱

規(guī)格：30m*0.32mm

型號：PEG-20M

應(yīng)用：亞麻籽油中脂肪酸的測定 氣相色譜法

浩瀚色譜（山東）應(yīng)用技術(shù)開發(fā)有限公司建立食用植物油脂中脂肪酸定量分析的氣相色譜內(nèi)標(biāo)法。方法采用氣相色譜內(nèi)標(biāo)法,內(nèi)標(biāo)物為c17:00甲酯,測定17種脂肪酸甲酯的相對校正因子（RCF）(以17:0為基準(zhǔn),即f17:0=1),分析9種市售新型植物油脂（三種茶油、三種橄欖油,1種亞麻籽油,2種紅花油）中脂肪酸構(gòu)成和含量,并對9種油中的脂肪酸構(gòu)成進行比較,分析油類脂肪酸含量的影響因素。以"克/100克可食部食物"來表示脂肪酸的含量。結(jié)果17種脂肪酸甲酯為8:0甲酯;10:0甲酯;12:0甲酯:14:0甲酯;16:0甲酯;16:1甲酯;18:0甲酯;18:1甲酯;18:2甲酯;18:3甲酯;20:0甲酯;20:4甲酯;20:5甲酯;22:0甲酯;22:1甲酯;22:6甲酯;24:0甲酯。實驗方法的回收率為85.06%,RSD=2.24%;精密度為RSD=2.42%。

亞麻籽油脂肪酸定量分析的氣相色譜  測試譜圖：



Gas Chromatography for the Quantitative Analysis of Flaxseed Oil Fatty Acids
Gas Chromatography for the Quantitative Analysis of Flaxseed Oil Fatty Acid Details:

Name: Capillary Column

Specification: 30m*0.32mm

Model: PEG-20M

Application: Determination of fatty acids in linseed oil gas chromatography

Haohan Chromatography (Shandong) Applied Technology Development Co., Ltd. established a gas chromatography internal standard method for the quantitative analysis of fatty acids in edible vegetable oils. The method uses gas chromatography internal standard method, the internal standard is c17:00 methyl ester, the relative correction factor (RCF) of 17 fatty acid methyl esters is determined (based on 17:0, that is, f17:0=1), and 9 kinds of analysis Fatty acid composition and content of new commercially available vegetable oils (three kinds of tea oil, three kinds of olive oil, one kind of linseed oil, two kinds of safflower oil), and compare the fatty acid composition of nine kinds of oils, and analyze oil fatty acids Factors affecting content. Use "g/100g of edible food" to express the content of fatty acids. Results 17 fatty acid methyl esters are 8:0 methyl ester; 10:0 methyl ester; 12:0 methyl ester: 14:0 methyl ester; 16:0 methyl ester; 16:1 methyl ester; 18:0 methyl ester; 18 : 1 methyl ester; 18:2 methyl ester; 18:3 methyl ester; 20:0 methyl ester; 20:4 methyl ester; 20:5 methyl ester; 22:0 methyl ester; 22:1 methyl ester; 22:6 Methyl ester; 24:0 Methyl ester. The recovery rate of the experimental method is 85.06%, RSD=2.24%; precision is RSD=2.42%.

Gas chromatographic test spectrum of linseed oil fatty acid quantitative analysis: